Experimental Study Of Zone Refining Of The Binary System Triphenyl Antimony Benzoic Acid

An experimental study on the zone refining of the binary system triphenyl antimony-benzoic acid is described. The isotope Sb124, which is a strong gamma emitter, was employed as a tracer; this allowed a rapid in situ nondestructive analysis, closely spaced experimental points, and the opportunity to study distribution as a function of varying experimental conditions. With the aid of computers (IBM 7090 and IBM 7044) apparent k's were calculated and the experimental data compared with those predicted from various mathematical models. (Author).

An experimental study on the zone refining of the binary system triphenyl antimony - naphthalene is described. The isotope Sb124, which is a strong gamma emitter, was employed as a tracer; this allowed a rapid in situ nondestructive analysis, closely spaced experimental points, and the opportunity to study distribution as a function of varying experimental conditions. With the aid of computers apparent k's were calculated and the experimental data compared with those predicted from various mathematical models. (Author).

The results of an experimental study of zone refining of the binary system triphenyl antimony-biphenyl are presented. The isotope Sb124, which is a strong gamma emitter, was employed as a tracer; this allowed a rapid in situ nondestructive analysis, closely spaced experimental points, and the opportunity to study distribution as a function of varying experimental conditions. With the aid of computers (IBM 7090 and IBM 7044) apparent (distribution coefficients) were calculated and the experimental data compared with those predicted from various mathematical models. (Author).

Thermoluminescence provides a method for studying properties of those crystalline imperfections which behave as electron traps and recombination centers in wide bandgap materials. This approach, however, has been used relatively little, possibly due to the fact that the shapes and intensities of thermoluminescent glow curves are functions of several experimental parameters and are often complicated by the overlapping of a number of individual glow peaks. In the present work, experimental parameters were isolated and some of their effects on thermoluminescent glow curves were analyzed. This yielded information on activation energies associated with trapping levels, the nature of the kinetics involved in electron transitions, and electron retrapping. A Type II-a diamond, which has a wide distribution of thermoluminescent glow peaks, was used in this work. (Author).