Infrared Spectroscopy In Conservation Science

This book provides practical information on the use of infrared (IR) spectroscopy for the analysis of materials found in cultural objects. Designed for scientists and students in the fields of archaeology, art conservation, microscopy, forensics, chemistry, and optics, the book discusses techniques for examining the microscopic amounts of complex, aged components in objects such as paintings, sculptures, and archaeological fragments. Chapters include the history of infrared spectroscopy, the basic parameters of infrared absorption theory, IR instrumentation, analysis methods, sample collection and preparation, and spectra interpretation. The authors cite several case studies, such as examinations of Chumash Indian paints and the Dead Sea Scrolls. The Institute’s Tools for Conservation series provides practical scientific procedures and methodologies for the practice of conservation. The series is specifically directed to conservation scientists, conservators, and technical experts in related fields.

Provides an introduction to those needing to use infrared spectroscopy for the first time, explaining the fundamental aspects of this technique, how to obtain a spectrum and how to analyse infrared data covering a wide range of applications. Includes instrumental and sampling techniques Covers biological and industrial applications Includes suitable questions and problems in each chapter to assist in the analysis and interpretation of representative infrared spectra Part of the ANTS (Analytical Techniques in the Sciences) Series.

Comprehensive Analytical Chemistry, Volume 84, the latest release in the Comprehensive Analytical Chemistry series, highlights new advances in the field, with this new volume presenting interesting chapters on the Current status of environmental monitoring, Physical principles of infrared, Chemical principles of infrared, Instrumentation and hardware, Data analysis, Sampling, Applications in water, Application in soil and sediments, Applications in ecology of animals and plants, Applications in air monitoring, Applications in contamination, Applications in marine environments, Advantages and pitfalls, and more. Provides the authority and expertise of leading contributors from an international board of authors Presents the latest release in the Damia Barcelo series Updated release includes the latest information on the Daniel Cozzolino

Comprehensive Analytical Chemistry, Volume 84, the latest release in the Comprehensive Analytical Chemistry series, highlights new advances in the field, with this new volume presenting interesting chapters on the Current status of environmental monitoring, Physical principles of infrared, Chemical principles of infrared, Instrumentation and hardware, Data analysis, Sampling, Applications in water, Application in soil and sediments, Applications in ecology of animals and plants, Applications in air monitoring, Applications in contamination, Applications in marine environments, Advantages and pitfalls, and more. Provides the authority and expertise of leading contributors from an international board of authors Presents the latest release in the Damia Barcelo series Updated release includes the latest information on the Daniel Cozzolino

SPECTROSCOPY FOR MATERIALS CHARACTERIZATION Learn foundational and advanced spectroscopy techniques from leading researchers in physics, chemistry, surface science, and nanoscience In Spectroscopy for Materials Characterization, accomplished researcher Simonpietro Agnello delivers a practical and accessible compilation of various spectroscopy techniques taught and used to today. The book offers a wide-ranging approach taught by leading researchers working in physics, chemistry, surface science, and nanoscience. It is ideal for both new students and advanced researchers studying and working with spectroscopy. Topics such as confocal and two photon spectroscopy, as well as infrared absorption and Raman and micro-Raman spectroscopy, are discussed, as are thermally stimulated luminescence and spectroscopic studies of radiation effects on optical materials. Each chapter includes a basic introduction to the theory necessary to understand a specific technique, details about the characteristic instrumental features and apparatuses used, including tips for the appropriate arrangement of a typical experiment, and a reproducible case study that shows the discussed techniques used in a real laboratory. Readers will benefit from the inclusion of: Complete and practical case studies at the conclusion of each chapter to highlight the concepts and techniques discussed in the material Citations of additional resources ideal for further study A thorough introduction to the basic aspects of radiation matter interaction in the visible-ultraviolet range and the fundamentals of absorption and emission A rigorous exploration of time resolved spectroscopy at the nanosecond and femtosecond intervals Perfect for Master and Ph.D. students and researchers in physics, chemistry, engineering, and biology, Spectroscopy for Materials Characterization will also earn a place in the libraries of materials science researchers and students seeking a one-stop reference to basic and advanced spectroscopy techniques.

Conservation Science is a rather innovative application of instrumental analysis with steadily increasing importance. Although the first attempts for preserving material from the cultural heritage on a scientific basis are found in the 19th century pioneer chemistry years, only the use of sophisticated physicochemical techniques results in effective identification and deterioration studies of monuments and objects, and in reliable intervention procedures. This volume allows to gain solid knowledge and improved skills on the ways separation schemes and diagnostic methodologies are applied in the safeguarding and authentication of tangible works of art; as well as on the modes of implementing novel safeguarding practices built on well-established principles – such as the use of laser in the decontamination of objects. All techniques are covered at a state-of-the-art level; while selected applications permit addressing major groups of materials and artefacts. Conservation Science is nowadays taught at master’s level in all developed countries, and museum laboratories increasingly adopt scientific approaches in their restoration initiatives. The book is intended as a valuable tool for students and professionals active in these frames. In addition, it provides an indispensable manual for participants in the specialized intensive courses, which are systematically offered by the authors under the auspices of the relevant European network.

This book will provide a survey of the major areas in which information derived from vibrational spectroscopy investigations and studies have contributed to the benefit of forensic science, either in a complementary or a unique way. This is highlighted by examples taken from real case studies and analyses of forensic relevance, which provide a focus for current and future applications and developments.

Materials in Art and Archaeology through their Infrared Spectra introduces students and professionals in archaeology, conservation, chemistry, and materials science to the world of archaeological and art materials. The infrared spectra of materials directly reflect their structures, whether amorphous or crystalline, color or colorless, polar (hydrophilic), or nonpolar (hydrophobic). Through this book, the reader is offered a top-down approach for interpreting the rich but often subtle information drawn from the infrared spectra of most materials in the above-described context and correlate them to their molecular geometry, their molecular environments, and, most importantly, their deterioration pathways that lead to their current condition.