Practical Polymer Analysis

The aim of this book is to familiarize the reader with the practical aspects of polymer analysis. A wealth of practical detail, including some detailed methods is included. The book covers not only the analysis of the main types of polymers and copolymers now in use commercially, but also the analysis of minor non-polymeric components of the polymer formulation, whether they be deliberately added, such as processing additives, or whether they occur adventitiously, such as moisture and residual monomers and solvent. A broad scheme for the examination of polymers is discussed in Chapter 2. Practically all of the major newer analytical techniques and many of the older classical techniques, have been used to examine polymers and their additive systems. As so many different polymers are now used commercially it is also advisable when attempting to identify a polymer to classify it by first separating it into pure polymeric and gross non polymeric fractions (Chapter Z) and then carrying out at least a qualitative elemental analysis and possible a quantitative analysis (Chapters 3 and 4) and then in some cases, depending on the elements found, to carry out functional group analysis (Chapters 6 and 9).

This book introduces the techniques used for the analysis of polymers. It covers the main aspects of polymer science and technology; identification, polymerization, molecular weight, structure, surface properties, degradation and mechanical properties. * Clear explanations of each analytical technique * Describes the application of techniques to the study of polymers * Encourages learning through numerous self-assessment questions and answers * Structured for flexible learning

Ein Praxisleitfaden der Polymeranalyse für alle, die sich in Polymerlabors mit Analytik, Qualitätskontrolle oder Produktentwicklung beschäftigen. Der Autor erläutert, aus seinem umfangreichen Erfahrungsschatz, welche Probleme in welchen Situationen auftreten können. Viele Fallstudien helfen bei der Anwendung der Erkenntnisse im Laboralltag. Mit einer umfangreichen Datensammlung zu physikalischen Eigenschaften von Polymeren! (07/00)

Designed to provide both an introduction and a practical guide to all aspects of polymer analysis, this book covers not only the various types of polymer now in commercial use, but also the minor non-polymeric components of their formulation, whether added deliberately, for example to improve service life, or present through the action of adventitious moisture, unreacted monomer, or excess solvent. All analytical techniques have been included, from the older, classical techniques of both elemental and functional group analysis, to the most modern physical techniques, including the various types of spectroscopy, gas chromatography-mass spectrometry, ozoneolysis, thermal methods, fractionation, and electron probe microanalysis. In each case, the technique is explained in detail, allowing the analyst to develop the considerable range of skills required to provide as complete a picture as possible of the polymer's structure. The extensive use of tables, the inclusion of numerous spectra and chemical formulae, and a comprehensive reference list ensure that this book will be of lasting use, for both the student and the practising analytical chemist.

MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.

Basics of Polymer, Volume II, demonstrates the scope of polymer testing. In addition, it introduces versatile methods of testing equipment effectively and clearly. In recent years, polymer testing has been extensively developed. Its utility has also been explored in detail, and areas of its practical application in the polymer industry have been added. Polymers, with their macromolecules, undergo a wide variety of phase changes during their processing. Due to this, the author discusses these important, useful, and instrumental techniques aimed at improving the quality of products. This book introduces the exceptionally promising instrumental methods that are of interest and relevance to technologists. Students interested in various aspects of instrumental techniques will also find the book useful. The instrumental techniques are discussed along with their possible applications to polymers. Looking to the future, it might be said that instrumental techniques will be, and should be, the methods for further research and study.

This undergraduate text provides an introduction to the physical principles behind the various techniques of polymer characterization without becoming deeply theoretical. It contains much detail of a practical nature, and special emphasis is placed on applications. Paper edition (unseen), $36. Annotation(c) 2003 Book News, Inc., Portland, OR (booknews.com)