Batch Chemical Process Integration

“Batch Chemical Process Integration: Analysis, Synthesis and Optimization” is an excellent source of information on state-of-the-art mathematical and graphical techniques for analysis, synthesis and optimization of batch chemical plants. It covers recent techniques in batch process integration with a particular focus on the capabilities of the mathematical techniques. There is a section on graphical techniques as well as performance comparison between graphical and mathematical techniques. Prior to delving into the intricacies of wastewater minimisation and heat integration in batch processes, the book introduces the reader to the basics of scheduling which is aimed at capturing the essence of time. A chapter on the synthesis of batch plants to highlight the importance of time in design of batch plants is also presented through a real-life case study. The book is targeted at undergraduates and postgraduate students, researchers in batch process integration, practising engineers and technical managers.

Written by a highly regarded author with industrial and academic experience, this new edition of an established bestselling book provides practical guidance for students, researchers, and those in chemical engineering. The book includes a new section on sustainable energy, with sections on carbon capture and sequestration, as a result of increasing environmental awareness; and a companion website that includes problems, worked solutions, and Excel spreadsheets to enable students to carry out complex calculations.

Batch chemical processes, so often employed in the pharmaceutical and agrochemical fields, differ significantly from standard continuous operations in the emphasis upon time as a critical factor in their synthesis and design. With this inclusive guide to batch chemical processes, the author introduces the reader to key aspects in mathematical modeling of batch processes and presents techniques to overcome the computational complexity in order to yield models that are solvable in near real-time. This book demonstrates how batch processes can be analyzed, synthesized, and designed optimally using proven mathematical formulations. The text effectively demonstrates how water and energy aspects can be incorporated within the scheduling framework that seeks to capture the essence of time. It presents real-life case studies where mathematical modeling of batch plants has been successfully applied.

Batch processes are used to manufacture many fine organic chemicals, and as such they can be considered to underpin much of the modern chemical industry. Despite widespread use and a consequent huge contribution to wealth creation, batch processes have attracted limited attention outside the user industries. Batch chemicals processing uses a number of core techniques and technologies, such as scheduling and sequence control, agitation and batch filtration. The combination of these technologies with often complex chemistry, the multi-purpose nature of much of this type of plant, the distinctive safety and environmental issues, and a fast moving commercial environment makes the development of a successful batch process a considerable challenge for the chemist or engineer. The literature on the topics covered in this book is fragmented and often not easily accessible, so this handbook has been written to address this problem and to bring together design and process analysis methods in the core areas of batch process design. By combining the science and pragmatism required in the development of successful batch processes this new book provides answers to real problems in an accessible and concise way. Written by an international team of authors drawn from industry, consulting and academe, this book is an essential part of the library of any chemist, technologist or engineer working on the development of new or existing batch processes.

Batch chemical processing has in the past decade enjoyed a return to respectability as a valuable, effective, and often preferred mode of process operation. This book provides the first comprehensive and authoritative coverage that reviews the state of the art development in the field of batch chemical systems engineering, applications in various chemical industries, current practice in different parts of the world, and future technical challenges. Developments in enabling computing technologies such as simulation, mathematical programming, knowledge based systems, and prognosis of how these developments would impact future progress in the batch domain are covered. Design issues for complex unit processes and batch plants as well as operational issues such as control and scheduling are also addressed.

Handbook of Process Integration (PI): Minimisation of Energy and Water Use, Waste and Emissions, Second Edition provides an up-to-date guide on the latest PI research and applications. Since the first edition published, methodologies and sustainability targets have developed considerably. Each chapter has been fully updated, with six new chapters added in this release, covering emissions, transport, water scarcity, reliability and maintenance, environmental impact and circular economy. This version also now includes worked examples and simulations to deepen the reader’s understanding. With its distinguished editor and international team of expert contributors, this book is an important reference work for managers and researchers in all energy and sustainability industries, as well as academics and students in Energy, Chemical, Process, and Environmental Engineering. Provides a fully updated handbook with six new chapters that reflect the latest research and applications on process integration Reviews a wide range of process design and integration topics, ranging from heat and utility systems to water, recycling, waste and hydrogen systems Covers equipment design and operability issues, with a strong extension to environmental engineering and suitability issues

This book deals with the design and integration of chemical processes, emphasizing the conceptual issues that are fundamental to the creation of the process. Chemical process design requires the selection of a series of processing steps and their integration to form a complete manufacturing system. The text emphasizes both the design and selection of the steps as individual operations and their integration. Also, the process will normally operate as part of an integrated manufacturing site consisting of a number of processes serviced by a common utility system. The design of utility systems has been dealt with in the text so that the interactions between processes and the utility system and interactions between different processes through the utility system can be exploited to maximize the performance of the site as a whole. Chemical processing should form part of a sustainable industrial activity. For chemical processing, this means that processes should use raw materials as efficiently as is economic and practicable, both to prevent the production of waste that can be environmentally harmful and to preserve the reserves of raw materials as much as possible. Processes should use as little energy as economic and practicable, both to prevent the build-up of carbon dioxide in the atmosphere from burning fossil fuels and to preserve reserves of fossil fuels. Water must also be consumed in sustainable quantities that do not cause deterioration in the quality of the water source and the long-term quantity of the reserves. Aqueous and atmospheric emissions must not be environmentally harmful, and solid waste to landfill must be avoided. Finally, all aspects of chemical processing must feature good health and safety practice. It is important for the designer to understand the limitations of the methods used in chemical process design. The best way to understand the limitations is to understand the derivations of the equations used and the assumptions on which the equations are based. Where practical, the derivation of the design equations has been included in the text. The book is intended to provide a practical guide to chemical process design and integration for undergraduate and postgraduate students of chemical engineering, practicing process designers and chemical engineers and applied chemists working in process development. Examples have been included throughout the text. Most of these examples do not require specialist software and can be performed on spreadsheet software. Finally, a number of exercises have been added at the end of each chapter to allow the reader to practice the calculation procedures.

Traditionally, process design and control system design are performed sequentially. It is only recently displayed that a simultaneous approach to the design and control leads to significant economic benefits and improved dynamic performance during plant operation. Extensive research in issues such as 'interactions of design and control', 'analysis and design of plant wide control systems', 'integrated methods for design and control' has resulted in impressive advances and significant new technologies that have enriched the variety of instruments available for the design engineer in her endeavour to design and operate new processes. The field of integrated process design and control has reached a maturity level that mingles the best from process knowledge and understanding and control theory on one side, with the best from numerical analysis and optimisation on the other. Direct implementation of integrated methods should soon become the mainstream design procedure. Within this context 'The Integration of Process Design and Control', bringing together the developments in a variety of topics related to the integrated design and control, will be a real asset for design engineers, practitioners and researchers. Although the individual chapters reach a depth of analysis close to the frontier of current research status, the structure of the book and the autonomous nature of the chapters make the book suitable for a newcomer in the area. The book comprises four distinct parts: Part A: Process characterization and controllability analysis Part B: Integrated process design and control ⊣ Methods Part C: Plant wide interactions of design and control Part D: Integrated process design and control ⊣ Extensions By the end of the book, the reader will have developed a commanding comprehension of the main aspects of integrated design and control, the ability to critically assess the key characteristics and elements related to the interactions between design and control and the capacity to implement the new technology in practice. * This book brings together the latest developments in a variety of topics related to integrated design and control. * It is a valuable asset for design engineers, practitioners and researchers. * The structure of the book and the nature of its chapters also make it suitable for a newcomer to the field.