Organic Functional Group Analysis

Organic Functional Group Analysis: Theory and Development attempts to symbolize the growth in functional groups analysis by using handpicked methods. Those methods are positioned to represent as many functional groups as possible. The book begins with the author referencing books about a quantitative organic analysis. Majority of the first few chapters highlight the oximation and carbonyl method, which support portions of Chapter 2 and the book's second half. The book then discusses the hydroxyl, amino, and alkoxysilanes groups. Chapters 3 and 4 showcase the strong analytical advantages in using base catalysis and acid catalysis with the same anhydride, while Chapters 5, 6, and 7 illustrate extremely useful functional group methods that have received impetus from research. The next chapters talk about the quantitative ring opening method and Diels-Alder addition method. Succeeding studies are about various compounds and its relevant subtopics. The text provides a very great reference for undergraduates and postgraduates of chemistry and its affiliated studies.

Describes the methods for identifying and measuring the amounts of organic constituents present in materials-organic compounds either in the pure state or in complex mixtures. Uses the functional groups as the analytical handle for measuring the compounds being studied, and shows interrelationships between methods.

Monographs in Organic Functional Group Analysis, Volume 3: Determination of Carboxylic Functional Groups focuses on the quantitative determination of acid chlorides, esters, carboxylic acids, anhydrides, lactones, and amides. The monograph first takes a look at the determination of carboxylic acids. Countercurrent and electrophoretic separation of organic acids; polarography of organic acids; acid-base equilibrium in non-aqueous media; and titrimetric determination of acids are discussed. The book also examines the determination of acid anhydrides, chlorides, and esters. The characteristics and composition of acid chlorides and anhydrides, as well as the saponification and spectroscopic methods used in the identification of esters, are presented. The book also evaluates the methods and use of Grignard’s reagent in the determination of amides. The text also presents an analysis of binary and ternary mixtures. Mixtures of acids and acid chlorides, differentiation of acids, mixtures of acids and esters, and mixtures of acids and amides are discussed. The monograph is a vital reference for readers interested in the quantitative determination of acid chlorides, esters, carboxylic acids, and other related compounds.

Organic Functional Group Analysis ...

Organic Functional Group Analysis deals with versatile and reliable chemical methods for the analysis of most of the more common organic functional groups. The minimum number of methods required to solve the maximum number of problems is presented. The scope and known limitations of each method are discussed so that analytical chemists can decide whether the method under consideration can be applied to their particular problem. The methods are either titrimetric or colorimetric in nature. This volume is comprised of 11 chapters and begins with an overview of the analytical methods used for organic functional groups, including both titrimetric and colorimetric methods. The discussion then turns to the properties of acids and bases; selection of the best acid-base method for a particular purpose; and some of the more useful acid-base methods. Subsequent chapters explore methods for the determination of nitrogen compounds such as amines and amides; carbonyl compounds and derivatives; hydroxyl compounds such as tertiary alcohols; unsaturated compounds; 1,2-epoxy compounds; esters and peroxides; carboxylic acid anhydrides; and sulfur compounds. This book is intended for analytical chemists.

Emphasises on contemporary applications and an intuitive problem-solving approach that helps students discover the exciting potential of chemical science. This book incorporates fresh applications from the three major areas of modern research: materials, environmental chemistry, and biological science.

Hydroxyl groups; Carbonyl proups; Carboxylic acids, salts, esters, amides, imides, chlorides, and anhydrides; Alkoxyl and oxyalkalene groups; Epoxide groups (oxirane oxygen); Organic peroxides; Unsaturation; Active hydrogen; Acetylenic hydrogen; Acetals, ketals, and vinyl ethers; Amino groups; Imino groups; Titanous, chromous, and ferrous reductions; Hydrazibes and hydrazides; Diazonius salts.