Spectroscopy Of Polymer Nanocomposites

Spectroscopy of Polymer Nanocomposites covers all aspects of the spectroscopic characterization of polymer nanocomposites. More than 25 spectroscopy characterization techniques – almost all used in materials science – are treated in the book, with discussion of their potentialities and limitations. By comparing the techniques with each other and presenting the techniques together with their specific application areas, the book provides scientists and engineers the information needed for solving specific problems and choosing the right technique for analyzing the material structure. From this, the dispersion structure of fillers, property relations and filler-polymer interactions can be determined, and, ultimately, the right materials can be chosen for the right applications. Besides the techniques and structure-property relations, aspects covered include: phase segregation of filler particles, filler agglomeration and deagglomeration, filler dispersion, filler-polymer interactions, surfaces and interfaces. The book also examines recent developments, as well as unresolved issues and new challenges, in the characterization of surfaces and interfaces in polymer nanocomposites. This handpicked selection of topics, and the combined expertise of contributors from industry, academia, government and private research organizations across the globe, make this survey an outstanding reference source for anyone involved in the field of polymer nanocomposites in academia or industry. Provides comprehensive coverage of spectroscopy techniques for analyzing polymer nanocomposites Enables researchers and engineers to choose the right technique and make better materials decisions in research and a range of industries Presents the fundamentals, information on structure-property relations, and all other aspects relevant for understanding spectroscopic analyses of nanoreinforced polymers and their applications

With its focus on the characterization of nanocomposites using such techniques as x-ray diffraction and spectrometry, light and electron microscopy, thermogravimetric analysis, as well as nuclear magnetic resonance and mass spectroscopy, this book helps to correctly interpret the recorded data. Each chapter introduces a particular characterization method, along with its foundations, and makes the user aware of its benefits, but also of its drawbacks. As a result, the reader will be able to reliably predict the microstructure of the synthesized polymer nanocomposite and its thermal and mechanical properties, and so assess its suitability for a particular application. Belongs on the shelf of every product engineer.

An insightful exploration of cutting-edge spectroscopic techniques in polymer characterization In Spectroscopic Techniques for Polymer Characterization: Methods, Instrumentation, Applications, a team of distinguished chemists delivers a comprehensive exploration of the vast potential of spectroscopic characterization techniques in polymer research. The book offers a concise outline of the principles, advantages, instrumentation, experimental techniques, and noteworthy applications of cutting-edge spectroscopy. Covering a wide range of polymers, from nylon to complex polymeric nanocomposites, the author presents recent developments in polymer science to polymer, analytical, and material chemists, assisting them in keeping track of the progress in modern spectroscopy. Spectroscopic Techniques for Polymer Characterization contains contributions from pioneers in modern spectroscopic techniques from around the world. The included materials bridge the gap between spectroscopists, polymer scientists, and engineers in academia and industry. The book also offers: A thorough introduction to the progress in spectroscopic techniques, including polymer spectroscopy and near-infrared spectroscopy Comprehensive explorations of topical polymers studied by spectroscopy, including polymer thin films, fluoropolymers, polymer solutions, conductive polymers Practical discussions of infrared imaging, near-infrared imaging, two-dimensional correlation spectroscopy, and far-ultraviolet spectroscopy In-depth examinations of spectroscopic studies of weak hydrogen bonding in polymers Spectroscopic Techniques for Polymer Characterization: Methods, Instrumentation, Applications is a must-read reference for polymer, analytical, and physical chemists, as well as materials scientists and spectroscopists seeking a one-stop resource for polymer characterization using spectroscopic analyses.

Polymer Nanocomposites for Energy Applications Explore the science of polymer nanocomposites and their practical use in energy applications In Polymer Nanocomposites for Energy Applications, a team of distinguished researchers delivers a comprehensive review of the synthesis and characterization of polymer nanocomposites, as well as their applications in the field of energy. Succinct and insightful, the book explores the storage of electrical, magnetic, and thermal energy and hydrogen. It also discusses energy generation by polymer-based solar cells. Finally, the authors present a life cycle analysis of polymer nanocomposites for energy applications and provide four real-world case studies where these materials have been successfully used. Readers will also find: Thorough introductions to the origins and synthesis of polymer materials In-depth discussions of the characterization of polymeric materials, including UV-visible spectroscopy Comprehensive explorations of a wide variety of polymer material applications, including in biotechnology and for soil remediation Fulsome presentations of polymer nanocomposites and their use in energy storage systems Perfect for materials and engineering scientists and polymer chemists, Polymer Nanocomposites for Energy Applications will also earn a place in the libraries of professionals working in the chemical industry.

Significant research has been done in polymeric nanocomposites and progress has been made in understanding nanofiller-polymer interface and interphase and their relation to nanocomposite properties. However, the information is scattered in many different publication media. This is the first book that consolidates the current knowledge on understanding, characterization and tailoring interfacial interactions between nanofillers and polymers by bringing together leading researchers and experts in this field to present their cutting edge research. Eleven chapters authored by senior subject specialists cover topics including: Thermodynamic mechanisms governing nanofiller dispersion, engineering of interphase with nanofillers Role of interphase in governing the mechanical, electrical, thermal and other functional properties of nanocomposites, characterization and modelling of the interphase Effects of crystallization on the interface, chemical and physical techniques for surface modification of nanocellulose reinforcements Electro-micromechanical and nanoindentation techniques for interface evaluation, molecular dynamics (MD) simulations to quantify filler-matrix adhesion and nanocomposite mechanical properties.

Clay–Polymer Nanocomposites is a complete summary of the existing knowledge on this topic, from the basic concepts of synthesis and design to their applications in timely topics such as high-performance composites, environment, and energy issues. This book covers many aspects of synthesis such as in- situ polymerization within the interlamellar spacing of the clays or by reaction of pristine or pre-modified clays with reactive polymers and prepolymers. Indeed, nanocomposites can be prepared at industrial scale by melt mixing. Regardless the synthesis method, much is said in this book about the importance of theclay pre-modification step, which is demonstrated to be effective, on many occasions, in obtaining exfoliated nanocomposites. Clay–Polymer Nanocomposites reports the background to numerous characterization methods including solid state NMR, neutron scattering, diffraction and vibrational techniques as well as surface analytical methods, namely XPS, inverse gas chromatography and nitrogen adsorption to probe surface composition, wetting and textural/structural properties. Although not described in dedicated chapters, numerous X-ray diffraction patterns of clay–polymer nanocomposites and reference materials are displayed to account for the effects of intercalation and exfoliations of layered aluminosilicates. Finally, multiscale molecular simulation protocols are presenting for predicting morphologies and properties of nanostructured polymer systems with industrial relevance. As far as applications are concerned, Clay–Polymer Nanocomposites examines structural composites such as clay–epoxy and clay–biopolymers, the use of clay–polymer nanocomposites as reactive nanocomposite fillers, catalytic clay-(conductive) polymers and similar nanocomposites for the uptake of hazardous compounds or for controlled drug release, antibacterial applications, energy storage, and more. The most comprehensive coverage of the state of the art in clay–polymer nanocomposites, from synthesis and design to opportunities and applications Covers the various methods of characterization of clay–polymer nanocomposites - including spectroscopy, thermal analyses, and X-ray diffraction Includes a discussion of a range of application areas, including biomedicine, energy storage, biofouling resistance, and more

Polymer Nanocomposites: Synthesis, Characterization, and Modeling examines the unique chemical and physical aspects associated with polymer based nanocomposite materials. The volume discusses the latest fundamental and applied research in the field of polymer nanocomposites as well as future directions for the development of high performance materials.

Raman Spectroscopy Applied to Polymer Composites and Nanocomposites summarizes, in a comprehensive manner, recent research accomplishments in this important area. The book offers an in-depth study of the current state-of-the-art, covering the fundamentals and recent experimental developments. Almost all the characterization techniques coupled in situ with Raman spectroscopy are discussed in detail. The book also covers various aspects of polymer applications, as well as related topics in polymer composites and nanocomposites. Filled polymers, reinforced plastics, thermoplastics, thermosets, elastomers, and rubbers are also discussed. The book is designed to address all aspects of Raman spectroscopy with respect to polymers and measurements, along with experimental conditions. It contains numerous case study examples to illustrate how Raman spectroscopy coupled in situ with more classical techniques can be useful to enhance material performance.