Advanced Distillation Technologies

Distillation has historically been the main method for separating mixtures in the chemical process industry. However, despite the flexibility and widespread use of distillation processes, they still remain extremely energy inefficient. Increased optimization and novel distillation concepts can deliver substantial benefits, not just in terms of significantly lower energy use, but also in reducing capital investment and improving eco-efficiency. While likely to remain the separation technology of choice for the next few decades, there is no doubt that distillation technologies need to make radical changes in order to meet the demands of the energy-conscious society. Advanced Distillation Technologies: Design, Control and Applications gives a deep and broad insight into integrated separations using non-conventional arrangements, including both current and upcoming process intensification technologies. It includes: Key concepts in distillation technology Principles of design, control, sizing and economics of distillation Dividing-wall column (DWC) – design, configurations, optimal operation and energy efficient and advanced control DWC applications in ternary separations, azeotropic, extractive and reactive distillation Heat integrated distillation column (HIDiC) – design, equipment and configurations Heat-pump assisted applications (MVR, TVR, AHP, CHRP, TAHP and others) Cyclic distillation technology – concepts, modeling approach, design and control issues Reactive distillation – fundamentals, equipment, applications, feasibility scheme Results of rigorous simulations in Mathworks Matlab & Simulink, Aspen Plus, Dynamics and Custom Modeler Containing abundant examples and industrial case studies, this is a unique resource that tackles the most advanced distillation technologies – all the way from the conceptual design to practical implementation. The author of Advanced Distillation Technologies, Dr. Ir. Anton A. Kiss, has been awarded the Hoogewerff Jongerenprijs 2013. Find out more (website in Dutch)...

This book describes the current state of the art in the retrofit of existing distillation processes using advanced distillation techniques. Highlighting concept and practical application rather than theory, it emphasizes the use of advanced process integration and intensification techniques, such as multi-effect distillation, heat pump assisted distillation, thermally coupled distillation, dividing wall column, reactive distillation, and innovative hybrid systems. As a thermal separation method, distillation is one of the most important and widely used technologies in the chemical process industry. While it has many advantages, one major drawback is its large energy requirement, which can significantly influence overall plant profitability. The increasing cost of energy has forced industry to reduce its energy requirement, but simultaneously there has been a need to increase capacity and output due to heightened demand. To accomplish this, the retrofit of distillation processes to increase efficiency and output has become a crucial issue. This book describes the use of advanced process integration and process intensification techniques to carry out effective distillation retrofit. Written by leading researchers in distillation process, process integration, process intensification, and process retrofit, the book presents a comprehensive review of contemporary advanced distillation techniques which can be employed in grass-root systems and retrofit. It is a valuable source of information for undergraduate and postgraduate students of chemical engineering, practicing process designers and chemical engineers.

Distillation: Equipment and Processes—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation equipment and processes. Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers Practical information on the newest development written by recognized experts Coverage of a huge range of laboratory and industrial distillation approaches Extensive references for each chapter facilitates further study

Low Grade Heat Driven Multi-effect Distillation and Desalination describes the development of advanced multi-effect evaporation technologies that are driven by low grade sensible heat, including process waste heat in refineries, heat rejection from diesel generators or microturbines, and solar and geothermal energy. The technologies discussed can be applied to desalination in remote areas, purifying produced water in oil-and-gas industries, and to re-concentrate process liquor in refineries. This book is ideal for researchers, engineering scientists, graduate students, and industrial practitioners working in the desalination, petrochemical, and mineral refining sectors, helping them further understand the technologies and opportunities that relate to their respective industries. For researchers and graduate students, the core enabling ideas in the book will provide insights and open up new horizons in thermal engineering. Focuses on advanced, yet practical, distillation technologies using low-grade sensible heat Explains the new design paradigm that must accompany the development of technologies Contains key experimental data that serves to prove the core concepts that underpin the new technologies Covers extensive thermo-economic analyses of the technologies, the price point for adoption, capital cost comparison with existing technologies, operating costs, and net present values

Neural Networks is an integral part in machine learning and a known tool for controlling nonlinear processes. The area is under rapid development and provides a tool for modelling and controlling of advanced processes. This book provides a comprehensive overview for modelling, simulation, measurement and control strategies for reactive distillations using neural networks.

After an overview of the fundamentals, limitations, and scope of reactive distillation, this book uses rigorous models for steady-state design and dynamic analysis of different types of reactive distillation columns and quantitatively compares the economics of reactive distillation columns with conventional multi-unit processes. It goes beyond traditional steady-state design that primarily considers the capital investment and energy costs when analyzing the control structure and the dynamic robustness of disturbances, and discusses how to maximize the economic and environmental benefits of reactive distillation technology.

Distillation: Operation and Applications—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation applications. Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers Practical information on the newest development written by recognized experts Coverage of a huge range of laboratory and industrial distillation approaches Extensive references for each chapter facilitates further study

THE FIRST BOOK OF ITS KIND ON DISTILLATION TECHNOLOGY The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly enhanced tower capacity and efficiency. With all these advances, one would expect the failure rate in distillation towers to be on the decline. In fact, the opposite is the case: the tower failure rate is on the rise and accelerating. Distillation Troubleshooting collects invaluable hands-on experiences acquired in dealing with distillation and absorption malfunctions, making them readily accessible for those engaged in solving today's problems and avoiding tomorrow's. The first book of its kind on the distillation industry, the practical lessons it offers are a must for those seeking the elusive path to trouble-free distillation. Distillation Troubleshooting covers over 1,200 case histories of problems, diagnoses, solutions, and key lessons. Coverage includes: * Successful and unsuccessful struggles with plugging, fouling, and coking * Histories and prevention of tray, packing, and internals damage * Lessons taught by incidents and accidents during shutdowns, commissioning, and abnormal operation * Troubleshooting distillation simulations to match the real world * Making packing liquid distributors work * Plant bottlenecks from intermediate draws, chimney trays, and feed points * Histories of and key lessons from explosions and fires in distillation towers * Prevention of flaws that impair reboiler and condenser performance * Destabilization of tower control systems and how to correct it * Discoveries from shutdown inspections * Suppression of foam and accumulation incidents A unique resource for improving the foremost industrial separation process, Distillation Troubleshooting transforms decades of hands-on experiences into a handy reference for professionals and students involved in the operation, design, study, improvement, and management of large-scale distillation.